3-Chloro-N-cyclohexylbenzamide
نویسندگان
چکیده
In the title mol-ecule, C(13)H(16)ClNO, the mean plane of the atoms in the -CONH- group forms a dihedral angle of 42.0 (4)° with the benzene ring plane. In the crystal structure, mol-ecules are linked by inter-molecular N-H⋯O hydrogen bonds, generating C(4) chains along [100].
منابع مشابه
4-Chloro-N-cyclohexylbenzamide
In the title compound, C(13)H(16)ClNO, the cyclo-hexyl ring adopts a chair conformation, with puckering parameters Q = 0.576 (3) Å, θ = 0.1 (3) and ϕ = 8 (15)°. In the crystal structure, inter-molecular N-H⋯O hydrogen bonds link mol-ecules into one-dimensional chains propagating in [010].
متن کاملSynthesis and Characterization of Some Lanthanide(III) Chloro Complexes Derived from 4[N-(4’-Hydroxy-3’-Methoxybenzalidene) Amino] Antipyrine Semicarbazone and 4[N-(3’,4’,5’-Trimethoxybenzalidene) Amino]Antipyrine Semicarbazone
Lanthanide(III) chloro complexes of 4[N-(4’-hydroxy-3’-methoxybenzalidene) amino] antipyrine semicarbazone (HMBAAPS) (I) and 4[N-(3’,4’,5’-trimethoxybenzalidene) amino] antipyrine semicarbazone (TMBAAPS) (II) with the general composition LnCl3.2L (Ln = La, Pr, Nd, Sm, Gd, Tb, Dy or Ho; L = HMBAAPS or TMBAAPS) are reported. All the complexes were synthesized in ethanolic medium and refluxed the ...
متن کاملN-Cyclohexylbenzamide
The structure of the title compound, C(13)H(17)NO, features an anti disposition of the N-H and carbonyl groups. The amide group is twisted with respect to the benzene ring [N-C(=O)-C-C torsion angle = -30.8 (4)°]. In the crystal, C(4) chains propagating in [100] are formed by inter-molecular N-H⋯O hydrogen bonds. Weak C-H⋯π inter-actions link the chains into sheets.
متن کاملA convenient method for 14C-labeling of N-(7-chloro-1- methyl-2-oxo-5-phenyl-2,3-dihydro-1Hbenzo[ e][1,4]diazepin-3-yl)thiophene-2-carboxamide as CCK-A antagonist
N-(7-chloro-1-methyl-2-oxo-5-phenyl-2,3-dihydro-1H-benzo[e][1,4]diazepin-3-yl)thiophene-2 carboxamide-[14C-carboxy] was prepared as part of a 6-step sequence from thiophene-2-carbonitrile -[cyano-14C] as a keysynthetic intermediate which has been synthesized from 2-iodothiophene and zinc [14C]-cyanide in thepresence of tetrakis (triphenylphosphine) palladium.
متن کامل2,4-Dichloro-N-cyclohexylbenzamide
In the title mol-ecule, C(13)H(15)Cl(2)NO, the cyclohexane ring adopts a chair conformation. The aromatic ring plane is oriented with respect to the N/O/C plane at a dihedral angle of 51.88 (7)°. In the crystal structure, inter-molecular N-H⋯O hydrogen bonds link the mol-ecules into infinite chains along the [010] direction.
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عنوان ژورنال:
دوره 65 شماره
صفحات -
تاریخ انتشار 2009